Spring 2002
M or W 1:30-5:30
OH-100 (Lecture) and OH-152 (Lab)
Instructors
Dr. C. Eugene Cain  Dr. Kristina L. Stensaas
OH 153 OH 149
Office Phone:  974-1404 Office Phone:  974-1402
cainece@millsaps.edu stenskl@millsaps.edu
Text: Macroscale and Microscale Organic Experiments  3rd Edition by Kenneth L. Williamson
Lab notebook:  A bound notebook will be supplied to you during laboratory. 
Goggles:  Safety goggles will be worn at all times in the laboratory. 
Objectives:   The primary objective of this course is to introduce students to the techniques, tools, and methods of the organic chemistry laboratory.  Students are encouraged to develop intuition and deepen their understanding of chemical concepts, master reporting skills, and reach reasonable conclusions based on experimental data.
Requirements:  Chemistry 2120 is to be taken concurrently.
Attendance:  Attendance is mandatory.  Pre-lab lectures are given at 1:30 p.m. during your regular lab session.  Students must be present in order to carry out the experiment scheduled for that week.  Laboratory work and experiments are to be completed during the regular lab periods.  Work at night or times outside of regularly scheduled lab periods will not be permitted.  If unusual circumstances indicate the need to attend the other regularly scheduled laboratory session, you must ask permission from your instructor beforehand.  E-mail messages received immediately prior to or after the laboratory are unacceptable! 
Safety: The Millsaps College Chemistry Department Safety Policy is attached to this syllabus.  Read this material carefully as it will be strictly enforced. 
Note:  Students with learning disabilities or other disabilities or special circumstances (pregnancy) need to contact the instructor after class to discuss individual needs for accomodations. 
Pre-Labs: Pre-Lab assignments are due at the beginning of your regularly scheduled laboratory period.  Computer based pre-lab assignments are to be completed and entered before 1:30 p.m. of the day you are scheduled for laboratory.
Notebook:   All experimental data will be entered directly into your notebook using ink.  Any results or statements in the notebook found to be in error should be marked through with a single straight line.  The date you start and complete an experiment must be recorded in the left-hand margin.  Refer to the attached sheet for further procedures in preparing laboratory records.  Notebooks must be turned in immediately after lab unless otherwise directed.
Grading: The course grade will be based on two exams (100 points each), weekly pre-labs or quizzes (10 points each), plus 6 experiments.  The point totals on individual experiments vary.  During the second half of the semester your status as a fledgling organic chemist is acknowledged and you will be given unknown organic compounds to identify.  Your acquired skills as an organic analyst will determine your grade during this exercise. Formal reports may be requested for certain experiments.
The tests will cover material learned in your laboratory work.  Several experiments will contain laboratory technique points which will be awarded as long as safety procedures, data reporting, and prudent laboratory practices are followed. 
Late Report Policy:  Late reports will lose 10% credit per day, including weekends.  Reports over one week late will constitute a missed lab.
Grading in this course will be on a curve with cut-off points no higher than those shown below.
 
A
94-100%
C+
76-79%
A-
90-93%
C
73-75%
B+
86-89%
C-
70-72%
B
83-85%
D+
66-69%
B-
80-82%
D
60-65%
F
below 60%
Honor Code:  Organic lab offers the opportunity for learning by individual team work and through collaboration.  Having taken the pledge of the Millsaps Honor Code, you will be expected to make clear to the instructor when the work is yours alone.  Pre-lab assignments are to be pledged individual work.  If the work is collaborative, as in experiments with partners, then the pledge of each student should indicate all those who contributed to the work. Please read the Academic Honor Code of Millsaps College which is posted in the Organic laboratory.
Changes: Changes to this syllabus are not anticipated, but if necessary they will be announced in class.
Schedule of Experiments for Spring 2002
Dates
(Mon. and Wed.)
Lab Text 
Experiment
January
14 and 16
Chapter 13
Introduction to Mass Spectrometry* and
Proton (1H) Nuclear Magnetic Resonance**
21 and 23
Chapter 13
Continue 1H NMR and discuss 13C NMR**
28 and 30
Chapter 13
Mass Spec., IR, and NMR Problem Solving
February
4 and 6
Chapter 38
Grignard Reaction
11 and 13
Chapter 28 
Nitration of Methyl Benzoate
Electrophilic Aromatic Substitution
18 and 20 Exam #1
25 and 27
Chapter 40
Esterification
March
4 and 6 
Chapter 37
Aldol Condensation
11 and 13  Spring Break
18 and 20 
Chapter 70
Qualitative Organic Analysis
Identification of  3 Unknown Compounds
25 and 27
Chapter 70
Unknowns
April
1 and 3
Chapter 70
Unknowns
8 and 10
Chapter 70
Unknowns
15 and 17
Chapter 70
Last Day for Unknowns/Results Due
22 and 24 Exam #2/Check-Out
* Read pages 441-451 in McMurry.
**Also read Chapter 13 in McMurry.
 
 
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