Chemistry 3400 Laboratory 200 Points Lab Meeting time: 1:00 – 4:00 p.m. Thursday [NO Make-UP Labs; No Late Lab Reports] Some of the computations required to analyze laboratory data will require the use of a computer and software, such as EXCEL. Pre-laboratory work will cover these procedures and will be conducted within the normal lab time. There will not be a formal laboratory meeting each week. The experiment will be done following completion of the indicated text chapters. Other time within the laboratory hours will be used for pre-labs, simulations, and computational training. Lab Reports are due at the next lab time unless otherwise indicated. Date Experiment/Activity and Location Lab Handouts are found under "Course Supplements" 1/17 No Lab Meeting 1/24 Lab1 Data Analysis [OH105] Read: Lab Reports, Q Test, Error Analysis Do: Excel Tutorial Experiment with: Uncertainty Calculator (using PV=nRT) 1/31 Lab2 - Report due next lab period Data Analysis with Excel [OH105] 2/07 Lab3 Heat of Neutralization [PCHEM Lab - FORMAL LAB REPORT] [Pre-Lab:http://www.chm.davidson.edu/ChemistryApplets/calorimetry/HeatOFNeutralization.html] 2/14 Lab4 Energy, Entropy, and Phase Changes [OH105] 2/21 Lab5 Thermodynamics Exercise [See "Course Supplements"] 2/28 Lab6 Electrochemistry [OH105] 3/06 Lab7 Acid/Base Titration [titr.exe]; Diff plot - Excel Technique will be discussed in lecture. *The Lab Report due date will be specified in lab 3/13 Lab8 Determination of an Equilibrium Constant [Formal Report] 3/20 Spring Break - No Lab 3/27 Lab9 Kinetics Experiment - Iodine Clock - ["Course Supplements"] Formal Lab Report using Data from Simulation; include Excel Analysis 4/03 No Lab this week 4/10 Lab10 "Course Supplements" - Molecular Modeling Exercise (Do Part I ONLY and submit Answers to Questions 1-5)] Read other material provided under "Lab 10". 4/17 Lab11 Molecular Modeling - "PC-SPARTAN Lab" Meet in Lab Behind my Office 2 Groups of Three: 1 p.m. and 2 p.m. 4/24 No Lab LABORATORY RULES Experimental work may be hazardous. Pay CLOSE attention to pre-labs and observe all safety precautions. ALWAYS wear safety glasses when in the lab. NEVER work in the lab alone. NEVER smoke, eat, or drink in the lab. ALWAYS dispose of waste appropriately – ask if you are uncertain. ALWAYS clean the lab before leaving. BE SURE you know where the fire extinguisher, first-aid kits, safety showers, eyewash fountains, and exits are. RECORDING LAB DATA AND THE LAB REPORT (1) Experiments will normally be performed in a group. You may share the duties BUT each person is responsible for all activities. Each person submits a lab report. (2) Neatness and organization are important. (3) For the Laboratory Report, evaluation of the experimental data will be required and standard procedures for data rejection (Q-test) and Confidence Interval should be used as appropriate. (4) The Lab Report is due 1 week after the experiment. NO EXTENSIONS. (5) BASIC FORMAT for Lab Report [typed and printed]: a. Title Page and Abstract b. Introduction c. Experimental Method d. Results[Tables and Graphics WILL enhance the report/improve your grade.] e. Discussion f. References (in proper form) g. Appendices See Other Information about the Lab Report Under "Course Supplements". LABORATORY GRADE Each Lab Report is Marked on a 10 Point Basis 20% for being present and performing the experiments 80% for Lab Reports